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  8. 2-Bromo-4-methylaniline, 99%, Thermo Scientific Chemicals

2-Bromo-4-methylaniline, 99%, Thermo Scientific Chemicals

Product Code. 11424904
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Quantity:
50 g
250 g
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Description

The N-(3, 5-Dichlorophenyl) naphthaldimine was obtained from the reaction of 2-hy- droxynaphthalene-l-carbaldehyde (0.01 mol) with a solution of 2-bromo-4-methylaniline (0.01 mol) in 40 ml of ethanol. Reaction of 2-bromo-4-methylaniline was quite clean, albeit 3,4-diaminotoluene was isolated just in 37% yield after flash chromatography on silica gel. The bromomethylquinoline starting material 16 was synthesized in two steps using an optimized process route by condensing 2-bromo-4-methylaniline.

This Thermo Scientific Chemicals brand product was originally part of the Alfa Aesar product portfolio. Some documentation and label information may refer to the legacy brand. The original Alfa Aesar product / item code or SKU reference has not changed as a part of the brand transition to Thermo Scientific Chemicals.

Applications
The N-(3, 5-Dichlorophenyl) naphthaldimine was obtained from the reaction of 2-hy- droxynaphthalene-l-carbaldehyde (0.01 mol) with a solution of 2-bromo-4-methylaniline (0.01 mol) in 40 ml of ethanol. Reaction of 2-bromo-4-methylaniline was quite clean, albeit 3,4-diaminotoluene was isolated just in 37% yield after flash chromatography on silica gel. The bromomethylquinoline starting material 16 was synthesized in two steps using an optimized process route by condensing 2-bromo-4-methylaniline.

Solubility
Insoluble in water.

Notes
Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Store away from strong oxidizing agents.
TRUSTED_SUSTAINABILITY

Chemical Identifiers

CAS 583-68-6
Molecular Formula C7H8BrN
Molecular Weight (g/mol) 186.052
MDL Number MFCD00007635
InChI Key UVRRJILIXQAAFK-UHFFFAOYSA-N
Synonym 2-bromo-p-toluidine, benzenamine, 2-bromo-4-methyl, 4-amino-3-bromotoluene, 2-bromo-4-methylbenzenamine, p-toluidine, 2-bromo, 2-bromo-4-methyl-phenylamine, 3-bromo-4-aminotoluene, 4-methyl-2-bromoaniline, 2-bromo-4-methyl aniline, 2-bromo-4-methyl-aniline
PubChem CID 11422
IUPAC Name 2-bromo-4-methylaniline
SMILES CC1=CC(=C(C=C1)N)Br

Specifications

Melting Point 14°C to 16°C
Density 1.494
Boiling Point 240°C to 242°C
Flash Point >110°C (230°F)
Odor Characteristic
Refractive Index 1.603
Quantity 250 g
UN Number UN2810
Beilstein 1931711
Solubility Information Insoluble in water.
Formula Weight 186.06
Percent Purity 99%
Chemical Name or Material 2-Bromo-4-methylaniline
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